Micro-Characterization of Indoor Deposited Particles Using FTIR, SEM-EDS, and XRD Techniques: A Case Study of a University Campus, Bangladesh

Abstract Micro-characterization of indoor atmospheric particles is essential for understanding atmospheric particle consequences on human health. In this study, the atmospheric particles were collected from inside the different buildings of KUET campus. The samples underwent characterization through...

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Main Authors: Mamun Mahmud, Kazi ABM Mohiuddin
Format: Article
Language:English
Published: Springer 2024-03-01
Series:Aerosol and Air Quality Research
Subjects:
Online Access:https://doi.org/10.4209/aaqr.230236
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author Mamun Mahmud
Kazi ABM Mohiuddin
author_facet Mamun Mahmud
Kazi ABM Mohiuddin
author_sort Mamun Mahmud
collection DOAJ
description Abstract Micro-characterization of indoor atmospheric particles is essential for understanding atmospheric particle consequences on human health. In this study, the atmospheric particles were collected from inside the different buildings of KUET campus. The samples underwent characterization through FTIR, SEM-EDS, and XRD techniques. Among the four sampled locations, the New Academic Building (NAB) had the highest rate of atmospheric particle deposition at 3.96 µg cm−2 day−1. The FTIR analysis indicated that the primary functional groups present across all samples were organic, specifically hydroxyl (-OH), aliphatic carbon (-CH2), carbonyl (-CO), and amino (-NH2) groups. The morphological analysis by SEM depicted the shape of indoor particles as angular, micro-flake, cubic, and irregular with the major chemical compositions of C, O, Al, Si, Ca, Na, Fe, and Mg of which Si and Fe were dominant in CEC and CEL sites which most likely originated from construction activities and dust from paved and unpaved roads. The average crystallinity of studied atmospheric particles was found to be a minimum of 27.3% at RH and a maximum of 64.5% at NAB sites and the corresponding crystalline size was 11.10 nm and 42.92 nm respectively. Quartz mineral in the inorganic fraction of atmospheric particles was found predominantly in every sample which most likely originates from soil erosion, construction activities and vehicular emissions. The outcome of this study will enhance our understanding of organic and inorganic compounds in atmospheric particles and their significance regarding radiative forcing, health impacts, and policy considerations for atmospheric particle sources.
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series Aerosol and Air Quality Research
spelling doaj-art-1e2c713974ab43e7b8336cb4ec1219ae2025-02-09T12:24:22ZengSpringerAerosol and Air Quality Research1680-85842071-14092024-03-0124511510.4209/aaqr.230236Micro-Characterization of Indoor Deposited Particles Using FTIR, SEM-EDS, and XRD Techniques: A Case Study of a University Campus, BangladeshMamun Mahmud0Kazi ABM Mohiuddin1Department of Civil Engineering, Khulna University of Engineering & TechnologyDepartment of Civil Engineering, Khulna University of Engineering & TechnologyAbstract Micro-characterization of indoor atmospheric particles is essential for understanding atmospheric particle consequences on human health. In this study, the atmospheric particles were collected from inside the different buildings of KUET campus. The samples underwent characterization through FTIR, SEM-EDS, and XRD techniques. Among the four sampled locations, the New Academic Building (NAB) had the highest rate of atmospheric particle deposition at 3.96 µg cm−2 day−1. The FTIR analysis indicated that the primary functional groups present across all samples were organic, specifically hydroxyl (-OH), aliphatic carbon (-CH2), carbonyl (-CO), and amino (-NH2) groups. The morphological analysis by SEM depicted the shape of indoor particles as angular, micro-flake, cubic, and irregular with the major chemical compositions of C, O, Al, Si, Ca, Na, Fe, and Mg of which Si and Fe were dominant in CEC and CEL sites which most likely originated from construction activities and dust from paved and unpaved roads. The average crystallinity of studied atmospheric particles was found to be a minimum of 27.3% at RH and a maximum of 64.5% at NAB sites and the corresponding crystalline size was 11.10 nm and 42.92 nm respectively. Quartz mineral in the inorganic fraction of atmospheric particles was found predominantly in every sample which most likely originates from soil erosion, construction activities and vehicular emissions. The outcome of this study will enhance our understanding of organic and inorganic compounds in atmospheric particles and their significance regarding radiative forcing, health impacts, and policy considerations for atmospheric particle sources.https://doi.org/10.4209/aaqr.230236Indoor air pollutionCrystalline silicaMicroplasticsFTIRSEM-EDSXRD
spellingShingle Mamun Mahmud
Kazi ABM Mohiuddin
Micro-Characterization of Indoor Deposited Particles Using FTIR, SEM-EDS, and XRD Techniques: A Case Study of a University Campus, Bangladesh
Aerosol and Air Quality Research
Indoor air pollution
Crystalline silica
Microplastics
FTIR
SEM-EDS
XRD
title Micro-Characterization of Indoor Deposited Particles Using FTIR, SEM-EDS, and XRD Techniques: A Case Study of a University Campus, Bangladesh
title_full Micro-Characterization of Indoor Deposited Particles Using FTIR, SEM-EDS, and XRD Techniques: A Case Study of a University Campus, Bangladesh
title_fullStr Micro-Characterization of Indoor Deposited Particles Using FTIR, SEM-EDS, and XRD Techniques: A Case Study of a University Campus, Bangladesh
title_full_unstemmed Micro-Characterization of Indoor Deposited Particles Using FTIR, SEM-EDS, and XRD Techniques: A Case Study of a University Campus, Bangladesh
title_short Micro-Characterization of Indoor Deposited Particles Using FTIR, SEM-EDS, and XRD Techniques: A Case Study of a University Campus, Bangladesh
title_sort micro characterization of indoor deposited particles using ftir sem eds and xrd techniques a case study of a university campus bangladesh
topic Indoor air pollution
Crystalline silica
Microplastics
FTIR
SEM-EDS
XRD
url https://doi.org/10.4209/aaqr.230236
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