Multi-scale structural evolution during simulated gelatinization process of sweet potato starch by heat-moisture treatment

The changes in properties and structures of raw sweet potato starch (RAW-SPS) and heat-moisture treatment (HMT) sweet potato starch (HMT-SPS) during gelatinization process (S1-S6) was investigated to elucidate the improvement effect of HMT on SPS. It was found that SPS exhibited the characteristics...

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Main Authors: Sijie Zhang, Weiguo Wu, Jihe Zhu, Junling Wu, Zengpeng Gan, Houqin Deng, Yu Zhang, Luyan Liao
Format: Article
Language:English
Published: Elsevier 2025-01-01
Series:Food Chemistry: X
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Online Access:http://www.sciencedirect.com/science/article/pii/S2590157524010113
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author Sijie Zhang
Weiguo Wu
Jihe Zhu
Junling Wu
Zengpeng Gan
Houqin Deng
Yu Zhang
Luyan Liao
author_facet Sijie Zhang
Weiguo Wu
Jihe Zhu
Junling Wu
Zengpeng Gan
Houqin Deng
Yu Zhang
Luyan Liao
author_sort Sijie Zhang
collection DOAJ
description The changes in properties and structures of raw sweet potato starch (RAW-SPS) and heat-moisture treatment (HMT) sweet potato starch (HMT-SPS) during gelatinization process (S1-S6) was investigated to elucidate the improvement effect of HMT on SPS. It was found that SPS exhibited the characteristics of pseudoplastic fluids, characterized by shear thinning and thixotropy, belonged to the C-type starch crystal. The gelatinization temperature of SPS was increased to 82.55 °C by HMT. HMT-SPS had better viscoelasticity in S3-S6. The particle size was smaller than that of RAW-SPS during the gelatinization process. The starch paste of S2 was gelatinized by heating at 95 °C, and the original crystalline structure of the starch was destroyed, where layered structure formed by recrystallization was observed. HMT-SPS showed a clear polarization cross, while disappeared after S2. HMT also improved the ordering degree. The results explained the mechanism of changes in HMT modified starch during the gelatinization process.
format Article
id doaj-art-a5c77d860b464866964eddb671fac059
institution Kabale University
issn 2590-1575
language English
publishDate 2025-01-01
publisher Elsevier
record_format Article
series Food Chemistry: X
spelling doaj-art-a5c77d860b464866964eddb671fac0592025-02-12T05:32:05ZengElsevierFood Chemistry: X2590-15752025-01-0125102123Multi-scale structural evolution during simulated gelatinization process of sweet potato starch by heat-moisture treatmentSijie Zhang0Weiguo Wu1Jihe Zhu2Junling Wu3Zengpeng Gan4Houqin Deng5Yu Zhang6Luyan Liao7College of Food Science and Technology, Hunan Agricultural University, Changsha 410128, ChinaCollege of Food Science and Technology, Hunan Agricultural University, Changsha 410128, ChinaSchool of Food and Pharmacy, Shanghai Zhongqiao Vocational and Technical University, Shanghai 201514, ChinaCollege of Food Science and Technology, Hunan Agricultural University, Changsha 410128, ChinaCollege of Food Science and Technology, Hunan Agricultural University, Changsha 410128, ChinaCollege of Food Science and Technology, Hunan Agricultural University, Changsha 410128, China; Hunan Province Key Laboratory of Food Science and Biotechnology, Changsha 410128, ChinaCollege of Food Science and Technology, Hunan Agricultural University, Changsha 410128, China; Hunan Province Key Laboratory of Food Science and Biotechnology, Changsha 410128, ChinaCollege of Food Science and Technology, Hunan Agricultural University, Changsha 410128, China; Hunan Province Key Laboratory of Food Science and Biotechnology, Changsha 410128, China; Corresponding author at: No.1, Nongda Road, Furong District, Changsha, Hunan 410128, China.The changes in properties and structures of raw sweet potato starch (RAW-SPS) and heat-moisture treatment (HMT) sweet potato starch (HMT-SPS) during gelatinization process (S1-S6) was investigated to elucidate the improvement effect of HMT on SPS. It was found that SPS exhibited the characteristics of pseudoplastic fluids, characterized by shear thinning and thixotropy, belonged to the C-type starch crystal. The gelatinization temperature of SPS was increased to 82.55 °C by HMT. HMT-SPS had better viscoelasticity in S3-S6. The particle size was smaller than that of RAW-SPS during the gelatinization process. The starch paste of S2 was gelatinized by heating at 95 °C, and the original crystalline structure of the starch was destroyed, where layered structure formed by recrystallization was observed. HMT-SPS showed a clear polarization cross, while disappeared after S2. HMT also improved the ordering degree. The results explained the mechanism of changes in HMT modified starch during the gelatinization process.http://www.sciencedirect.com/science/article/pii/S2590157524010113Heat-moisture treatmentSweet potato starchGelatinization stageStructure changes
spellingShingle Sijie Zhang
Weiguo Wu
Jihe Zhu
Junling Wu
Zengpeng Gan
Houqin Deng
Yu Zhang
Luyan Liao
Multi-scale structural evolution during simulated gelatinization process of sweet potato starch by heat-moisture treatment
Food Chemistry: X
Heat-moisture treatment
Sweet potato starch
Gelatinization stage
Structure changes
title Multi-scale structural evolution during simulated gelatinization process of sweet potato starch by heat-moisture treatment
title_full Multi-scale structural evolution during simulated gelatinization process of sweet potato starch by heat-moisture treatment
title_fullStr Multi-scale structural evolution during simulated gelatinization process of sweet potato starch by heat-moisture treatment
title_full_unstemmed Multi-scale structural evolution during simulated gelatinization process of sweet potato starch by heat-moisture treatment
title_short Multi-scale structural evolution during simulated gelatinization process of sweet potato starch by heat-moisture treatment
title_sort multi scale structural evolution during simulated gelatinization process of sweet potato starch by heat moisture treatment
topic Heat-moisture treatment
Sweet potato starch
Gelatinization stage
Structure changes
url http://www.sciencedirect.com/science/article/pii/S2590157524010113
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